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Figure 11
Synthesis of ethyl ketopentenoate (EKP) via Lewis acid-catalyzed allylation of ethyl glyoxylate followed by Dess-Martin oxidation. Abbreviations: dichloromethane: DCM; ethyl hydroxypentenoate: EHP; 3-oxo-1λ5-benzo[d][1,2]iodaoxole-1,1,1(3H)-triyl triacetate: Dess-Martin periodinane; and room temperature: RT.
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